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MLZ
Lichtenbergstr.1
85748 Garching
Ralph Gilles
I am a physicist and heading the research group “Advanced Materials” with expertise in neutron scattering methods for studying energy materials as high-temperature alloys and batteries. At FRM II, I was working as an instrument scientist to design, built and brought in commission the structure powder diffractometer SPODI and the small-angle scattering instrument SANS-1 dedicated for materials science and magnetism at Heinz Maier-Leibnitz Zentrum (MLZ) in Garching, near Munich, Germany. In my group methods as diffraction, small-angle scattering, imaging, neutron depth profiling and neutron induced prompt gamma activation analysis are applied mainly for alloy and battery research. I authored over 160 peer-reviewed articles (37 as first author)on topics ranging from instrumentation at large scale facilities, alloy development, thin films, ceramics over to in-situ and operando studies on batteries. Furthermore, I am the industrial coordinator for industrial use of scientific instruments at the Heinz Maier-Leibnitz Zentrum.
Curriculum Vitae
since 2015 | Head of Advanced Materials group |
since 2012 | Group coordinator of the Materials Science group at Heinz Maier-Leibnitz Zentrum (MLZ) |
since 2005 | Coordinator for the industrial use of scientific instruments at the research neutron source Heinz Maier-Leibnitz (FRM II) |
2011-2020 | Head of the Materials Science Laboratory (X-ray diffraction, Small-angle X-ray scattering, DSC, microscopy, sample preparation etc.) |
2003-2015 | Instrument responsible for the Small-Angle Neutron Scattering instrument SANS-1 at FRM II in Garching |
1998-2003 | Instrument responsible for the Structure Powder Diffractometer SPODI at FRM II in Garching |
1995-1998 | Instrument responsible for the Small-Angle Neutron Scattering instrument V4 at Hahn-Meitner Institute in Berlin |
2004 | Habilitation in Materials Science – Superalloys and Neutron Scattering, University of Darmstadt |
1995 | Phd in Physics (Crystallography) – Thin films, University of Bonn |
1990 | Diploma in Physics, University of Bonn |
Selected Publications
Journal Article
Monitoring the precipitation of the hardening phase in the new VDM® Alloy 780 by in-situ high-temperature small-angle neutron scattering, neutron diffraction and complementary microscopy techniques
Journal of alloys and compounds 928, 167203 - (2022) [10.1016/j.jallcom.2022.167203]
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Journal Article
Cracking during High-Temperature Deformation of a High-Strength Polycrystalline CoNi-Base Superalloy
Metals 12(9), 1520 - (2022) [10.3390/met12091520]
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Journal Article
Near-Surface and Bulk Dissolution Behavior of γ′ Precipitates in Nickel-Based VDM® Alloy 780 Studied with In-Situ Lab-Source and Synchrotron X-ray Diffraction
Metals 12(7), 1067 - (2022) [10.3390/met12071067]
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Journal Article
Influence of pressure and temperature on the electrolyte filling of lithium-ion cells: Experiment, model and method
Journal of power sources 517, 230668 - (2022) [10.1016/j.jpowsour.2021.230668]
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Journal Article
Detection of hydrate plugs inside submarine pipelines using neutrons
Nondestructive testing and evaluation 36, 1 - 13 (2022) [10.1080/10589759.2021.1990284]
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Journal Article
Morphology–Ionic Conductivity Relationship in Polymer–Titania Hybrid Electrolytes for Lithium-Ion Batteries
ACS applied energy materials 4(12), 13438 - 13443 (2021) [10.1021/acsaem.1c03393]
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Journal Article
Effects of Polymer Coating Mechanics at Solid‐Electrolyte Interphase for Stabilizing Lithium Metal Anodes
Advanced energy materials 0, 2103187 (2021) [10.1002/aenm.202103187]
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Journal Article
Structure and Microstructure of Advanced Materials Characterized by Neutron Diffraction
Materials science forum 1016, 1404 - 1410 (2021) [10.4028/www.scientific.net/MSF.1016.1404]
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Journal Article
Deformation Mechanisms in Ni-Based Superalloys at Room and Elevated Temperatures Studied by In Situ Neutron Diffraction and Electron Microscopy
Metals 11(5), 719 (2021) [10.3390/met11050719] special issue: "Advances in Superalloys and High Temperature Intermetallics"
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Journal Article
TaC Precipitation Kinetics during Cooling of Co‐Re Base Alloys
Advanced engineering materials 23(11), adem.202100129 (2021) [10.1002/adem.202100129]
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Journal Article
Impact of Silicon Content within Silicon-Graphite Anodes on Performance and Li Concentration Profiles of Li-Ion Cells using Neutron Depth Profiling
Journal of the Electrochemical Society 168(2), 020519 - (2021) [10.1149/1945-7111/abe1db]
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Journal Article
Combining SANS and VSANS to Extend Q-Range for Morphology Investigation of Silicon-Graphite Anodes
Surface investigation, x-ray, synchrotron and neutron techniques 14(S1), S156 - S160 (2020) [10.1134/S1027451020070368]
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Journal Article
How Neutrons Facilitate Research into Gas Turbines and Batteries from Development to Engineering Applications
Journal of surface investigation 14(S1), S69 - S74 (2020) [10.1134/S1027451020070162]
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Journal Article
In Situ Neutron Diffraction Study of Ni Addition in Co–Re–Cr High-Temperature Alloys and Influence on Phase Transformations
Journal of surface investigation 14(S1), S179 - S184 (2020) [10.1134/S1027451020070071]
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Journal Article
A Liquid Electrolyte-Based Lithium-Ion Battery Cell Design for Operando Neutron Depth Profiling
Journal of the Electrochemical Society 167(10), 100554 - (2020) [10.1149/1945-7111/ab9b20]
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Journal Article
SEI Growth Impacts of Lamination, Formation and Cycling in Lithium Ion Batteries
Batteries 6(2), 21 - (2020) [10.3390/batteries6020021]
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Journal Article
Enhancing the High-Temperature Strength of a Co-Base Superalloy by Optimizing the gamma/gamma' Microstructure
Metals 10(3), 321 - (2020) [10.3390/met10030321]
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Journal Article
Li-ion half-cells studied operando during cycling by small-angle neutron scattering
Journal of applied crystallography 53(1), 210 - 221 (2020) [10.1107/S160057671901714X]
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Journal Article
HRTEM analysis of the high-temperature phases of the newly developed high-temperature Ni-base superalloy VDM 780 Premium
Journal of alloys and compounds 814, 152157 - (2020) [10.1016/j.jallcom.2019.152157]
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Journal Article
Effect of Cr and Ni on the microstructural evolution in Co–Re–Cr–Ni alloys
International journal of materials research 110(12), 1092 - 1104 (2019) [10.3139/146.111855]
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Journal Article
Influence of the Cell Format on the Electrolyte Filling Process of Lithium‐Ion Cells
Energy technology 0, ente.201801108 (2019) [10.1002/ente.201801108]
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Journal Article
Linear and Nonlinear Aging of Lithium-Ion Cells Investigated by Electrochemical Analysis and In-Situ Neutron Diffraction
Journal of the Electrochemical Society 166(16), A3908 - A3917 (2019) [10.1149/2.1271915jes]
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Journal Article
Low‐Temperature Charging and Aging Mechanisms of Si/C Composite Anodes in Li‐Ion Batteries – An Operando Neutron Scattering Study
ChemSusChem 12, 1 (2019) [10.1002/cssc.201903139]
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Journal Article
Monitoring the Lithium Concentration across the Thickness of Silicon-Graphite Electrodes during the First (De-)Lithiation
Journal of the Electrochemical Society 166(8), A1408 - A1411 (2019) [10.1149/2.0581908jes]
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Journal Article
Combined Small-Angle X-ray and Neutron Scattering Restraints in Molecular Dynamics Simulations
Journal of chemical theory and computation 15(8), 4687 - 4698 (2019) [10.1021/acs.jctc.9b00292]
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Contribution to a conference proceedings/Report/Contribution to a book
Study of Phase Distribution on Alloy UNS N07718 in Different Hardening Conditions and Its Relationship with Hydrogen Embrittlement Susceptibility
NACE - International Corrosion Conference Series
Corrosion Conference and Expo 2019, NACE2019, NashvilleNashville, United States, 24 Mar 2019 - 28 Mar 2019
Houston, Texas : National Assoc. of Corrosion Engineers International 13025: 1 - 14 (2019)
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Journal Article
Proton conductivity in a hureaulite-type compound, Mn$_{5}$[(PO$_{4}$)$_{2}$(PO$_{3}$(OH))$_{2}$](HOH)$_{4}$
Journal of solid state chemistry 277, 290 - 302 (2019) [10.1016/j.jssc.2019.06.029]
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Journal Article
Contrast Matched SANS for Observing SEI and Pore Clogging in Silicon-Graphite Anodes
Journal of the Electrochemical Society 166(6), A1051 - A1054 (2019) [10.1149/2.0781906jes]
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Book/Proceedings
In Situ Characterization at High Temperature of VDM Alloy 780 Premium to Determine Solvus Temperatures and Phase Transformations Using Neutron Diffraction and Small-Angle Neutron Scattering
TMS 2019 Annual Meeting & Exhibition, TMS2019, San Antonio, TexasSan Antonio, Texas, USA, 10 Mar 2019 - 14 Mar 2019
Cham : Springer International Publishing, The Minerals, Metals & Materials Series (2019) [10.1007/978-3-030-05749-7_3]
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Journal Article
Rapid electrolyte wetting of lithium-ion batteries containing laser structured electrodes: in situ visualization by neutron radiography
The international journal of advanced manufacturing technology 102(9–12), 2769–2778 (2019) [10.1007/s00170-019-03347-4]
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Journal Article
Differentiation of γ′- and γ″- precipitates in Inconel 718 by a complementary study with small-angle neutron scattering and analytical microscopy
Acta materialia 163, 28 - 39 (2019) [10.1016/j.actamat.2018.10.014]
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Journal Article
Erratum to “Inhomogeneity and relaxation phenomena in the graphite anode of a lithium-ion battery probed by in situ neutron diffraction” [J. Power Sources 361 (2017) 54–60]
Journal of power sources 377, 189 - (2018) [10.1016/j.jpowsour.2017.11.095]
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Journal Article
Beyond Ni-base superalloys: Influence of Cr addition on Co-Re base alloys strengthened by nano-sized TaC precipitates
Physica / B Condensed matter B 551, 1 - 5 (2018) [10.1016/j.physb.2017.11.059]
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Journal Article
In Situ Characterization at Elevated Temperatures of a New Ni-Based Superalloy VDM-780 Premium
Metallurgical and materials transactions / A Physical metallurgy and materials science A 49(9), 4373 - 4381 (2018) [10.1007/s11661-018-4761-6]
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Journal Article
High-Temperature Stability of Phases in Boron Containing Co-Re Alloys for Gas Turbine Applications
Acta physica Polonica / A A 134(3), 829 - 837 (2018) [10.12693/APhysPolA.134.829]
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Journal Article
Characterization of anisotropic pores and spatially oriented precipitates in sintered Mo-base alloys using small-angle neutron scattering
Journal of applied crystallography 51(6), 1706 - 1714 (2018) [10.1107/S1600576718014474]
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Journal Article
Materials science applications of Neutron Depth Profiling at the PGAA facility of Heinz Maier-Leibnitz Zentrum
Materials characterization 146, 127 - 134 (2018) [10.1016/j.matchar.2018.09.030]
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Journal Article
The new neutron depth profiling instrument N4DP at the Heinz Maier-Leibnitz Zentrum
Nuclear instruments & methods in physics research / A Accelerators, spectrometers, detectors and associated equipment Section A 911, 30 - 36 (2018) [10.1016/j.nima.2018.09.113]
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Journal Article
Quantifying the Distribution of Electrolyte Decomposition Products in Silicon-Graphite Electrodes by Neutron Depth Profiling
Connections / Athena papers Athena papers [...] 165(10), A2340 - A2348 (2018) [10.1149/2.1341810jes]
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Journal Article
Conductivity and Morphology Correlations of Ionic-Liquid/Lithium-Salt/Block Copolymer Nanostructured Hybrid Electrolytes
ACS applied energy materials 1(2), 666 - 675 (2018) [10.1021/acsaem.7b00173]
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Journal Article
Introduction to Electrochemical Impedance Spectroscopy as a Measurement Method for the Wetting Degree of Lithium-Ion Cells
Connections / Athena papers Athena papers [...] 165(14), A3249 - A3256 (2018) [10.1149/2.0081814jes]
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Journal Article
Matrix Transformation in Boron Containing High-Temperature Co–Re–Cr Alloys
Metals and materials international 24(5), 934 - 944 (2018) [10.1007/s12540-018-0121-8]
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Journal Article
Creep deformation of Co-Re-Ta-C alloys with varying C content–investigated in-situ by simultaneous synchrotron radiation diffraction
Materials science and engineering / A Structural materials : properties, microstructure and processing properties, microstructure and processing 719, 124 - 131 (2018) [10.1016/j.msea.2018.02.009]
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Journal Article
Additional Phases at High Boron Content in High-Temperature Co–Re–Cr Alloys
Metals 8(8), 621 - (2018) [10.3390/met8080621]
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Journal Article
In Situ Neutron Diffraction Study of Lithiation Gradients in Graphite Anodes during Discharge and Relaxation
Journal of the Electrochemical Society 165(9), A1846 - A1856 (2018) [10.1149/2.1231809jes]
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Journal Article
Electrodeposited Na$_2$Ni[Fe(CN)$_6$] Thin-Film Cathodes Exposed to Simulated Aqueous Na-Ion Battery Conditions
The journal of physical chemistry <Washington, DC> / C 122(16), 8760 - 8768 (2018) [10.1021/acs.jpcc.8b00395]
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Journal Article
Coexistence of Two Cubic-Lattice Co Matrices at High Temperatures in Co-Re-Cr-Ni Alloy Studied by Neutron Diffraction
Advances in materials science and engineering 2018, 1 - 6 (2018) [10.1155/2018/5410871]
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Journal Article
Aging in 18650-type Li-ion cells examined with neutron diffraction, electrochemical analysis and physico-chemical modeling
Journal of energy storage 17, 383 - 394 (2018) [10.1016/j.est.2018.03.016]
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Journal Article
Visualization of electrolyte filling process and influence of vacuum during filling for hard case prismatic lithium ion cells by neutron imaging to optimize the production process
Journal of power sources 380, 126 - 134 (2018) [10.1016/j.jpowsour.2018.01.081]
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Journal Article
Ageing and Water-Based Processing of LiFeMnPO$_4$ Secondary Agglomerates and Its Effects on Electrochemical Characteristics
Energies 10(12), 2135 - (2017) [10.3390/en10122135]
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Journal Article
Gas Evolution and Capacity Fading in LiFe$_x$Mn$_{1-x}$PO$_4$/Graphite Cells Studied by Neutron Imaging and Neutron Induced Prompt Gamma Activation Analysis
Journal of the Electrochemical Society 164(14), A3943 - A3948 (2017) [10.1149/2.0011802jes]
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Journal Article
Inhomogeneity and relaxation phenomena in the graphite anode of a lithium-ion battery probed by in situ neutron diffraction
Journal of power sources 361, 54 - 60 (2017) [10.1016/j.jpowsour.2017.06.060]
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Journal Article
Calibrating SANS data for instrument geometry and pixel sensitivity effects: access to an extended Q range
Journal of applied crystallography 50(5), 1382 - 1394 (2017) [10.1107/S1600576717011463]
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Journal Article
Cycling capacity recovery effect: A coulombic efficiency and post-mortem study
Journal of power sources 365, 327 - 338 (2017) [10.1016/j.jpowsour.2017.08.090]
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Journal Article
Influence of Particle Morphologies of LiFePO4 on Water- and Solvent-Based Processing and Electrochemical Properties
Sustainability 9(6), 888 - (2017) [10.3390/su9060888]
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Journal Article
The influence of C/Ta ratio on TaC precipitates in Co-Re base alloys investigated by small-angle neutron scattering
Acta materialia 132, 354 - 366 (2017) [10.1016/j.actamat.2017.04.029]
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Journal Article
Aging behavior of lithium iron phosphate based 18650-type cells studied by in situ neutron diffraction
Journal of power sources 345, 85 - 96 (2017) [10.1016/j.jpowsour.2017.01.134]
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Journal Article
Lithium plating in lithium-ion batteries investigated by voltage relaxation and in situ neutron diffraction
Journal of power sources 342, 17 - 23 (2017) [10.1016/j.jpowsour.2016.12.032]
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Journal Article
First-cycle defect evolution of Li$_{1−x}$Ni$_{1/3}$Mn$_{1/3}$Co$_{1/3}$O$_2$ lithium ion battery electrodes investigated by positron annihilation spectroscopy
Journal of power sources 336, 224 - 230 (2016) [10.1016/j.jpowsour.2016.10.050]
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Journal Article
In situ visualization of the electrolyte solvent filling process by neutron radiography
Journal of power sources 331, 267 - 276 (2016) [10.1016/j.jpowsour.2016.09.037]
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Journal Article
Effect of composition on the matrix transformation of the Co-Re-Cr-Ta-C alloys
Metals and materials international 22(4), 562 - 571 (2016) [10.1007/s12540-016-5697-2]
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Journal Article
Evolution of strain-induced hafnium carbides in a molybdenum base Mo–Hf–C alloy studied by small-angle neutron scattering and complementary methods
Journal of alloys and compounds 688, 619 - 631 (2016) [10.1016/j.jallcom.2016.06.282]
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Journal Article
Stability of TaC precipitates in a Co–Re-based alloy being developed for ultra-high-temperature applications
Journal of applied crystallography 49(4), 1253 - 1265 (2016) [10.1107/S1600576716009006]
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Journal Article
The new small-angle neutron scattering instrument SANS-1 at MLZ—characterization and first results
Nuclear instruments & methods in physics research / A 832, 297 - 305 (2016) [10.1016/j.nima.2016.06.105]
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Journal Article
Current status of Co-Re-based alloys being developed to supplement Ni-based superalloys for ultra-high temperature applications in gas turbines
Kovové materiály 53(04), 287 - 294 (2016) [10.4149/km_2015_4_287]
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Journal Article
Neutron Tomography and Radiography on a Sodium Metal Halide Cell under Operating Conditions
Journal of the Electrochemical Society 163(6), A838 - A845 (2016) [10.1149/2.0181606jes]
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Journal Article
GISAXS and TOF-GISANS studies on surface and depth morphology of self-organized TiO$_2$ nanotube arrays: model anode material in Li-ion batteries
Journal of applied crystallography 48, 444-454 (2015) [10.1107/S1600576715002204]
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Journal Article
In Operando Small-Angle Neutron Scattering (SANS) on Li-Ion Batteries
Journal of the Electrochemical Society 162(2), A3116 - A3125 (2015) [10.1149/2.0181502jes]
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Journal Article
Battery research as progress pacemaker
Neutron news 26(1), 29 - 32 (2015) [10.1080/10448632.2015.996026]
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Journal Article
In Situ Spatially Resolved Neutron Diffraction of a Sodium Metal Halide Battery
Journal of the Electrochemical Society 162(3), A384 - A391 (2015) [10.1149/2.0421503jes]
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Journal Article
Aging Analysis of Graphite/LiNi$_{1/3}$Mn$_{1/3}$Co$_{1/3}$O$_2$ Cells Using XRD, PGAA, and AC Impedance
Journal of the Electrochemical Society 162(14), A2737 - A2746 (2015) [10.1149/2.0721514jes]
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Journal Article
In Situ Neutron Diffraction Characterization of Phases in Co-Re-Based Alloys at High Temperatures
Acta physica Polonica / A 128(4), 684 - 688 (2015) [10.12693/APhysPolA.128.684]
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Journal Article
Neutron and synchrotron probes in the development of Co-Re-based alloys for next generation gas turbines with an emphasis on the influence of boron additives
Journal of applied crystallography 47(4), 1417 - 1430 (2014) [10.1107/S1600576714013624]
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Journal Article
Lithium plating in lithium-ion batteries at sub-ambient temperatures investigated by in situ neutron diffraction
Journal of power sources 271, 152 - 159 (2014) [10.1016/j.jpowsour.2014.07.168]
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Journal Article
Investigations of early stage precipitation in a tungsten-rich nickel-base superalloy using SAXS and SANS
Journal of alloys and compounds 612, 90-97 (2014-00-) [10.1016/j.jallcom.2014.05.154]
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Journal Article
Effects of size reduction on the structure and magnetic properties of core–shell Ni3Si/silica nanoparticles prepared by electrochemical synthesis
Journal of alloys and compounds 584, 119-127 (2014-00-) [10.1016/j.jallcom.2013.09.035]
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Journal Article
Application of In Situ Neutron and X-Ray Measurements at High Temperatures in the Development of Co-Re-Based Alloys for Gas Turbines
Metallurgical and materials transactions / A 44, 22-30 (2013-01-) [10.1007/s11661-012-1363-6]
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Journal Article
Co-Re-based alloys a new class of material for gas turbine applications at very high temperatures
Advances in materials research 1(3), 205-219 (2012) [10.12989/amr.2012.1.3.205]
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Journal Article
Determination of phase compositions in ceramics from Gobi desert using complementary diffraction techniques
Journal of radioanalytical and nuclear chemistry (2012-11-) [10.1007/s10967-012-2325-6]
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Journal Article
The Hexagonal Close-Packed (HCP) ⇆ Face-Centered Cubic (FCC) Transition in Co-Re-Based Experimental Alloys Investigated by Neutron Scattering
Metallurgical and materials transactions / A 43, 1834-1844 (2012-00-) [10.1007/s11661-011-1058-4]
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Journal Article
Stability of phases at high temperatures in CoRe based alloys being developed for ultra-high temperature applications
Journal of physics / Conference Series 340, 012052 (2012-00-) [10.1088/1742-6596/340/1/012052]
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Journal Article
Spatially Resolved Phase Analysis in Sodium Metal Halide Batteries: Neutron Diffraction and Tomography
Journal of the Electrochemical Society 159, A1827-A1833 (2012-00-) [10.1149/2.058211jes]
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Journal Article
Investigation of metal-matrix composite containing liquid-phase dispersion
Journal of physics / Conference Series 340, 012098 (2012-00-) [10.1088/1742-6596/340/1/012098]
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Journal Article
Co-Re-based Alloys a New Class of Material for Gas Turbine Applications at Very High Temperatures
Advanced engineering materials 1, 205-219 (2012-00-) [10.12989/amr.2013.1.3.205]
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Contribution to a book
<i>In Situ</i> Investigation with Neutrons on the Evolution of γ ' Precipitates at High Temperatures in a Single Crystal Ni-Base Superalloy
Zug : Scitec Publ., Advanced materials research 278, 42-47 (2011-07-) [10.4028/www.scientific.net/AmR.278.42]
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Beyond Ni-based superalloys: Development of CoRe-based alloys for gas turbine applications at very high temperatures
International journal of materials research 102, 1125-1132 (2011-09-) [10.3139/146.110563]
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Analysis of antiphase domain growth in ternary FeCo alloys after different cooling rates and annealing treatments using neutron diffraction and positron annihilation
Journal of alloys and compounds 509, 195-199 (2011-00-) [10.1016/j.jallcom.2010.09.075]
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Investigation of phase transformations by in-situ neutron diffraction in a Co–Re-based high temperature alloy
Materials letters 64, 2608-2611 (2010-08-) [10.1016/j.matlet.2010.08.066]
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Probing the Relationship of Long-Range Order in Nanodomain FeCo Alloys with Ternary Additions Using Neutron Diffraction
Metallurgical and materials transactions / A 41, 1144-1150 (2010-05-) [10.1007/s11661-009-9933-y]
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Industrial Applications at the FRM II
Neutron news 21, 13-15 (2010-00-) [10.1080/10448632.2010.519629]
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Dependence of small-angle neutron scattering contrast on the difference in thermal expansions of phases in two-phase alloys
Journal of applied crystallography 42, 981-989 (2009-00-) [10.1107/S0021889809035353]
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The measurement of internal strain in core–shell Ni 3 Si(Al)–SiO x nanoparticles
Nanotechnology 20, 245704 (2009-00-) [10.1088/0957-4484/20/24/245704]
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New sources and instrumentation for neutrons in biology
Chemical physics 345, 133-151 (2008-00-) [10.1016/j.chemphys.2008.02.030]
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Microstructural characterisation of a Ni–Fe-based superalloy by in situ small-angle neutron scattering measurements
Journal of physics / Condensed matter 20, 104220-104228 (2008-00-) [10.1088/0953-8984/20/10/104220]
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Scientific Review: The Structure Powder Diffractometer SPODI
Neutron news 18, 23 - 26 (2007-00-) [10.1080/10448630701623251]
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Monte Carlo simulations of the new Small-Angle Neutron Scattering instrument SANS-1 at the Heinz Maier-Leibnitz Forschungsneutronenquelle
Journal of applied crystallography 40, s428 - s432 (2007-00-)
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Characterization of core-shell nanoparticles by small angle neutron scattering
Applied physics / A 88, 277 (2007-00-) [10.1007/s00339-007-4008-7]
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Phase analysis and lattice mismatches in superalloys DT706 and Inconel 706
Physica / B 385-386, 594 (2006-00-) [10.1016/j.physb.2006.06.108]
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Neutron and X-ray diffraction measurements on micro- and nano-sized precipitates embedded in a Ni-based superalloy and after their extraction from the alloy
Acta materialia 54, 1307-1316 (2006-00-) [10.1016/j.actamat.2005.11.004]
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First test measurements at the new structure powder diffractometer (SPODI) at the FRM-II
Zeitschrift für Kristallographie / Supplements 2006, 183-188 (2006-00-) [10.1524/zksu.2006.suppl_23.183]
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Characterization of nanoporous superalloy by SANS
Physica / B 385-386, 626 - 629 (2006-00-) [10.1016/j.physb.2006.06.118]
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Ni 3 Si(Al)/a-SiO x core–shell nanoparticles: characterization, shell formation, and stability
Nanotechnology 17, 4195-4203 (2006-00-) [10.1088/0957-4484/17/16/033]
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The concept of the new small-angle scattering instrument SANS-1 at the FRM-II
Physica / B 385-386, 1174-1176 (2006-00-) [10.1016/j.physb.2006.05.403]
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Microstructural characterization of a modified 706-type Ni-Fe superalloy by small-angle neutron scattering and electron microscopy
Metallurgical and materials transactions / A 36, 3439-3450 (2005-00-) [10.1007/s11661-005-0017-3]
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Neutron scattering, a powerful tool in material science exemplary on superalloys
International journal of materials research 96, 4 325-334 (2005-00-)
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Novel type of neutron image plates based on KCl:Eu$^{2+}$–LiF
Physica / B 350(1-3), E861 - E864 (2004) [10.1016/j.physb.2004.03.223]
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Monte Carlo simulations of various instrument configurations of the new structure powder diffractometer (SPODI)
Physica / B 350(1-3), E671 - E673 (2004) [10.1016/j.physb.2004.03.182]
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Nanocrystalline Ni 3 Al-type intermetallic phase powder from Ni-base superalloys
Nanotechnology 15, 648-657 (2004-00-) [10.1088/0957-4484/15/5/042]
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Small-Angle Neutron Scattering: A Tool for Microstructural Investigation of High-Temperature Materials
Materials science forum 426-432, 755 - 760 (2003-00-) [10.4028/www.scientific.net/MSF.426-432.755]
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SMALL-ANGLE SCATTERING, A TOOL TO CHARACTERIZE Ni-BASE SUPERALLOYS AT HIGH TEMPERATURE
Acta crystallographica / A A58 (Supplement), C26 (2002)
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A new detector system for the structure powder diffractometer SPODI at the FRM-II in Garching
Applied physics / A 74, S154-S156 (2002-00-) [10.1007/s003390201753]
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Structure and ionic conductivity in doped LaGaO 3
Applied physics / A 74, 966 (2002-00-) [10.1007/s003390101168]
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Untersuchungen an Nickelbasis-Superlegierungen mit Neutronen-, Röntgen- und Synchrotronstrahlung
Zeitschrift für Kristallographie / Supplements 20, 2 (2002-00-)
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Status of the new structure powder diffractometer (SPODI) at the FRM-II in Garching
Applied physics / A 74, 148-150 (2002-00-) [10.1007/s003390201739]
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A new method of Debye-Scherrer pattern integration on two-dimensional detectors, demonstrated for the new structure powder diffractometer (SPODI) at the FRM-II in Garching
Applied physics / A 74, 1477 - 1479 (2002-00-) [10.1007/s003390201432]
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SANS examination of precipitate microstructure in the creep-exposed single-crystal Ni-base superalloy SC16
Applied physics / A 74, 1083 (2002-00-) [10.1007/s003390101195]
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In situ SANS investigation of precipitate microstructure at elevated temperatures in Re-rich Ni-base superalloy
Applied physics / A 74, 1074 (2002-00-) [10.1007/s003390201681]
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Neutron-, X-ray- and electron-diffraction measurements for the determination of ?/? ? lattice misfit in Ni-base superalloys
Applied physics / A 74, s1446-s1448 (2002-00-) [10.1007/s003390201742]
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The Concept of the New Structure Powder Diffractometer (SPODI) at the FRM-II in Garching
Materials science forum 378-381, 282-287 (2001-00-) [10.4028/www.scientific.net/MSF.378-381.282]
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Determination of γ′ solution temperature in Re-rich Ni-base superalloy by small-angle neutron scattering
Journal of applied crystallography 34, 541--548 (2001-00-) [10.1107/S0021889801004708]
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Complexation properties of 1,3-dialkoxycalix[4]arene-crown derivatives: a SANS study
Physica / B 276-278, 384 (2000-00-) [10.1016/S0921-4526(99)01575-6]
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Concept of the new thermal single crystal diffractometer at FRM-II
Physica / B 276-278, 77-78 (2000-00-) [10.1016/S0921-4526(99)01344-7]
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Silver Behenate as a Standard for Instrumental Resolution and Wavelength Calibration for Small Angel Neutron Scattering
Materials science forum 321-324, 264 (2000-00-) [10.4028/www.scientific.net/MSF.321-324.264]
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The new structure powder diffractometer at the FRM-II in Garching
Physica / B 276-278, 87-88 (2000-00-) [10.1016/S0921-4526(99)01371-X]
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Structural studies of the 30S subunit of ribosomes Thermus thermophilus by small-angle neutron and X-ray scattering
Journal of applied crystallography 33, 515 (2000-00-) [10.1107/S0021889800098009]
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Non-destructive SANS study of creep-tested single-crystal Ni-base superalloy CMSX3
Physica / B 276-278, 890 (2000-00-) [10.1016/S0921-4526(99)01541-0]
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Evaluation procedure for anisotropic SANS
Journal of applied crystallography 33, 834 (2000-00-) [10.1107/S002188980009974X]
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Dr. habil. Ralph Gilles
Technische Universität München
Heinz Maier-Leibnitz Zentrum (MLZ)
Head of Advanced Materials Group
Lichtenbergstr. 1
85748 Garching
Phone: +49 (0)89 289-14665
E-Mail: ralph.gilles@frm2.tum.de
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