MLZ is a cooperation between:

Technische Universität München> Technische Universität MünchenHelmholtz-Zentrum Hereon> Helmholtz-Zentrum Hereon
Forschungszentrum Jülich> Forschungszentrum Jülich

MLZ is a member of:

LENS> LENSERF-AISBL> ERF-AISBL

MLZ on social media:

Logo

MLZ (eng)

Lichtenbergstr.1
85748 Garching

STRESS-SPEC

Materials science diffractometer

Insrumentscheme STRESS-SPEC Insrumentscheme STRESS-SPEC

In response to the development of new materials and the application of materials and components in new technologies, the direct measurement, calculation, and evaluation of textures and residual stresses has gained worldwide significance in recent years.

STRESS-SPEC, the materials science diffractometer, is located at the thermal beam tube SR-3 and can easily be configured either for texture analysis or strain measurements.

The set-up utilises three different monochromators: Ge(511), bent silicon Si(400), and pyrolitic graphite PG(002). This selection of monochromators and the possibility to automatically vary the take-off angles from 2θM = 35º to 110º allows us to find a good compromise between resolution and intensity for each measuring problem.

The gauge volume defining optical system of primary and secondary slits is designed with regard to the reproducibility of geometrical alignment and sturdiness. Instead of the slits, a set of radial collimators is available to define the gauge volume.

Samples can be aligned using theodolites and a camera system. In addition, the possibility of scanning surfaces of components offline using a CMM scanner is available.

Typical applications
Residual stress analysis [1]
  • Industrial components
  • Welds, additive manufactured samples
  • Superalloys
  • Strain mapping
  • Surface measurements from 150 µm possible [2]
Texture determination [3]
  • Global textures
  • Local textures
  • Strain pole figures
  • FHWM pole figures
Structural applications
  • Phase transformation dynamics
  • Spatially resolved phase analysis (e.g. batteries)

[1] Hofmann, M. et al., Physica B 385, 1035 (2006).
[2] Saroun, J. et al., J. Appl. Cryst. 46, 628 (2013).
[3] Brokmeier, H.-G. et al., NIM-A 642, 87 (2011).

Sample environment
  • xyz-table
    • Capacity 300 kg, travel xy = ±120 mm, z = 300 mm, accuracy ~ 10 µm
  • Load frame
    • +/-50 kN, heatable to 1000°C (in air), rotabale
    • +/-100 kN, heatable to 1500°C (vacuum)
  • Full circle Eulerian cradle (max. load 5 kg)
  • ¼ circle Eulerian cradle for heavy samples
  • Standard sample environment (e.g. furnace, cryostat)
  • Quenching & deformation dilatometer

A positioning system consisting of a Stäubli 6-axes robotic arm for texture and strain measurements (payload up to 30 kg) can be mounted instead of the standard sample table. It offers more flexibility than an Eulerian cradle and can also be used as an automatic sample changer for texture measurements [4]. A camera-based metrology system tracks the sample position [5].

[4] Randau, C. et al., NIM-A 794, 67 (2015).
[5] Landesberger et al., Sensors 24(9), 2703 (2024).

Technical data
Primary beam
  • Beam tube SR-3
  • Thermal neutrons
  • Collimators (‘in-pile’) 15’, 25’, open
Monochromators
  • Ge(511), Si(400), PG(002)
  • M 35° – 110° continuous
  • Wavelength 1 Å – 2.4 Å; (2.5 Å-1 < Q < 10.5 Å-1)
Possible slit size – Residual stress
  • Primary slit: automatically continuously variable up to 7 × 17 mm2 (W x H)
  • Secondary slit: continuously variable up to 15 mm
  • Radial collimators – incoming beam (FOV = 1 mm, 2 mm, 5 mm)
  • Radial collimators – diffracted beam (FOV = 0.5 mm, 1 mm, 2 mm, 5 mm, 10 mm)
Possible slit size – Textures
  • Primary slit: max. 30 × 40 mm2 (W x H)
  • Secondary slit: continuously variable up to 15 mm or open
Detector
  • 3He-PSD, 25 × 25 cm2; 256 × 256 pixels
Software

STeCa2 [6]
STeCa2 is the standard software tool for analysing the 2D-detector data of STRESS-SPEC. Besides display functionalities, various functions for integration and Bragg peak refinement are available. In addition, one can generate and visualise the pole figures from texture measurements. The software is available for Linux or Windows and can be downloaded from the web page of the Computing Group

DISEMM (Diffraction assisted mechanical modelling) [7]
The software DISEMM is designed to analyse diffraction data from in-situ loading experiments to obtain diffraction elastic and single-crystal elastic constants and to describe the mechanical behaviour by the elasto-plastic self-consistent modelling. DISEMM offers a variety of grain-to-grain interaction models and integrates texture and multi-phase alloys. The software is currently available for Windows. The DISEMM software can be downloaded here, with the corresponding manual here.

STRESSFIT [8, 9]
is a Python package for fitting neutron residual strain scanning data. The primary objective is to restore intrinsic lattice strain distributions measured by neutron diffraction. In an experiment, this distribution is smeared by the finite spatial resolution of the instrument. Measured strains are also affected by so-called pseudo-strains, which generally arise from an inhomogeneous sampling of the material. The best known is the surface effect, which occurs when the nominal gauge volume of the instrument is only partly immersed under the sample surface. This gives rise to peak shifts (pseudo strains) of similar magnitude as the intrinsic strain. The Python package can be reached here (https://github.com/NPLtools/stressfit), as well as the respective available documentation.

[6] Randau, C. et al., J. Appl. Cryst. 44, 641 (2011).
[7] Heldmann, A. et al., J. Appl. Cryst. 52, 1144 (2019).
[8] Rebelo Kornmeier, J. et al. Materials Characterization, 154, 53 (2019).
[9] Šaroun, J. et al., Physica B: Condensed Matter 551, 468 (2018).

Instrument scientists

Dr. Michael Hofmann
Phone: +49 (0)89 289-14744
E-mail: michael.hofmann@frm2.tum.de

Dr. Weimin Gan
Phone: +49 (0)89 158860-766
E-mail: weimin.gan@hzg.de

STRESS-SPEC
Phone: +49 (0)89 289-14814

Operated by

TUM

GEMS

Funding

News

Tracing the hydrogen

Tracing the hydrogen

Read more
Successful ErUM-Pro proposals

Successful ErUM-Pro proposals

Read more
Let's quench!

Let's quench!

Read more

Publications

Find the latest publications regarding STRESS-SPEC in our publication database iMPULSE:

impulse.mlz-garching.de

Citation of the instrument

Heinz Maier-Leibnitz Zentrum. (2015). STRESS-SPEC: Materials science diffractometer. Journal of large-scale research facilities, 1, A6. http://dx.doi.org/10.17815/jlsrf-1-25

For citation please always include the DOI.

Instrument control

Gallery

STRESS-SPEC_01
STRESS-SPEC_01
© W. Schürmann, TUM
STRESS-SPEC_02
STRESS-SPEC_02

Radial collimator setup

© MLZ
STRESS-SPEC_03
STRESS-SPEC_03

Robot at STRESS-SPEC holding a copper tube for combined texture and strain measurements

© MLZ
STRESS-SPEC_04
STRESS-SPEC_04

Resolution function for different monochromator options

© MLZ
STRESS-SPEC_05
STRESS-SPEC_05

Robot with camera-based tracking system

© MLZ

MLZ is a cooperation between:

Technische Universität München> Technische Universität MünchenHelmholtz-Zentrum Hereon> Helmholtz-Zentrum Hereon
Forschungszentrum Jülich> Forschungszentrum Jülich

MLZ is a member of:

LENS> LENSERF-AISBL> ERF-AISBL

MLZ on social media: