MLZ is a cooperation between:
> Technische Universität München
> Helmholtz-Zentrum Hereon
> Forschungszentrum Jülich
MLZ is a member of:
> LENS
> ERF-AISBL
MLZ on social media:
MLZ (eng)
Lichtenbergstr.1
85748 Garching
Physics laboratory
The Phyics Laboratory of TUM provides scientists with techniques for analysis and preparation of samples for subsequent neutron scattering experiments. An x-ray diffractometer for phase determination of powder and solid samples, in-situ battery measurements and for thin film systems is available. Furthermore, a differential scanning calorimeter and a bi-potentiostat are available. A wide range of machines for polishing, cutting, etching or annealing are available for sample preparation purposes.
Please get in touch with the Physics laboratory two to three weeks in advance the measurement so that the equipment can be prepared for you. You can check the current bookings in the Calendar.
Note: Access to the physics laboratory can only be granted after a safety traning has been performed. Please email to Physics laboratory for any questions.
Equipment:
Analytic instruments:
- phase and structure analysis, thin films
- solid, poweder and thin films
- reflection and transmission measurements
- x-ray tubes: Cu (λ = 1.541 Å), Mo (λ = 0.711 Å)
- angular range 2θ = -9° … 120°, d2θ = 0.005°
- detectors: GaliPIX3D (2d), X’Celerator (1d), Scintillator (0d)
- optics: monochromator (Cu), parallel mirror (Cu), focussing mirror (Mo)
- sample stages: reflection – transmission spinner, eulerian cradle
- vacuum/temperatur stage: T = 25°C … 1600°C with inert gas (Anton Paar HTK 16N)
coming soon
Technical specifications- x-ray tube: Cu (λ = 1.541 Å)
- angular range 2θ
- detecotors: Dectris Mythen (1d), Scintillator (0d)
coming soon
Technical specifications- x-ray tube: Cu (λ = 1.541 Å)
- angular range 2θ
- optics: parallel beam mirror
- detector: Scintillator (0d)
(outsourced to Prof. Müller-Buschbaum, TUM Physik E13)
- SAXS: Pilatus 2D detector 84 × 34 mm²
- WAXS: 1D wide angle detector, 2θ = 18° … 30°
- In-situ annealing of solid-, liquid- or powder samples T = -20° C … +300° C.
- Perkin Elmer DSC 8500: T = -180°C … +550°C, dT = ± 0.05°C
- Setaram Evotherm µDSC Evo3: T = -20°C … +120°C, dT = ± 0.001°C
- cyclic voltammetry I = 1 nA … 400 mA, dI = ± 760 pA, 5 µV, 20 µs
- impedance spectroscopy 10 µHz – 1 MHz
- 4 A und 100 A current boosters
- bright-, darkfield, transmission, reflection, multi focus
- polarization-, phase-, differential interference contrast
Preparation instruments:
- ceramic tube max. 1500 °C
- vacuum < 10-4 mbar, inter gas (N2, Ar)
temperature range: T = 30 °C … 200 °C, dT = 1 K
inner dimensions: 40 cm x 34 cm x 40 cm (lxwxh)
Presi BRILLANT 200 – corundum wheel saw
ATM OPAL 410 – resin sample hot embedding
ATM SAPHIR 520 – polishing machine
Contact:
Bookings
E-mail: physicslab@frm2.tum.de
Dr. Markos Skoulatos (head)
Phone: +49 (0)89 289 – 14668
E-mail: markos.skoulatos@frm2.tum.de
Teodora Kennel
Phone: +49 (0)89 289 – 10757
E-mail: teodora.kennel@frm2.tum.de
Alexander Book
Phone: +49 (0)89 289 – 12156
E-mail: alexander.book@frm2.tum.de
Matthias Wauro
Phone +49 (0)89 289 – 14917
E-mail: matthias.wauro@frm2.tum.de
Laboratory: UXB building, room 2.5.04
MLZ is a cooperation between:
> Technische Universität München> Helmholtz-Zentrum Hereon
> Forschungszentrum Jülich
MLZ is a member of:
> LENS> ERF-AISBL
MLZ on social media: