Physics laboratory

coming soon

Available options

• DC Resistance
• AC Resistance (ETO)
• Vibrating Sample Magnetometer (VSM)
• AC Susceptibility (ACMS II)
• Heat Capacity
• Horizontal Rotator for Transport Measurements
• Pressure Cells for Magnetometry (1.3 GPa) and Transport Measurements (2.7 GPa)
• Dilution Refrigerator (50 mK – 4 K) for AC Susceptibility, Heat Capacity, Electrical Transport (ETO/Resistivity)
• Synchronous Source and Measure System M81 SSM from LakeShore (DC/AC transport)

• phase and structure analysis
• solid, powder and thin films
• reflection and transmission measurements

• x-ray tubes: Cu (λ = 1.541 Å), Mo (λ = 0.711 Å)
• angular range 2θ = -9° … 120°, d2θ = 0.005°
• detectors: GaliPIX3D (2d), X’Celerator (1d), Scintillator (0d)
• optics: monochromator (Cu), parallel mirror (Cu), focussing mirror (Mo)
• sample stages: reflection – transmission spinner, eulerian cradle
• vacuum/temperatur stage: T = 25°C … 1600°C with inert gas (Anton Paar HTK 16N)

coming soon

• x-ray tube: Cu (λ = 2.290 Å)
• angular range 2θ
• 1/4-Circle eulerian cradle (χ = -3° .. 90°, ψ = 0 .. 360°)
• XYZ-Table (X = ± 75 mm, Y = ± 75 mm, Z = 0 .. 13 mm)
• detector: Dectris Mythen 1K (1d)

• thickness, density, roughness (thin films), phase identification
• thin films, powders

• x-ray tube: Cu (λ = 1.541 Å)
• angular range 2θ = -10° … 160°, d2θ = 0.003°
• optics: parallel beam mirror (Göbelmirror)
• stages: Reflectometer stage, powder spinner (Transmission)
• detector: Scintillator (0d)

(outsourced to Prof. Müller-Buschbaum, TUM Physik E13)

• SAXS: Pilatus 2D detector 84 × 34 mm²
• WAXS: 1D wide angle detector, 2θ = 18° … 30°
• In-situ annealing of solid-, liquid- or powder samples T = -20° C … +300° C.

• Perkin Elmer DSC 8500: T = -180°C … +550°C, dT = ± 0.05°C
• Setaram Evotherm µDSC Evo3: T = -20°C … +120°C, dT = ± 0.001°C

• cyclic voltammetry I = 1 nA … 400 mA, dI = ± 760 pA, 5 µV, 20 µs
• impedance spectroscopy 10 µHz – 1 MHz
• 4 A und 100 A current boosters

• bright-, darkfield, transmission, reflection, multi focus
• polarization-, phase-, differential interference contrast

• ceramic tube max. 1500 °C
• vacuum < 10^-4 mbar, inter gas (N₂, Ar)

temperature range: T = 30 °C … 200 °C, dT = 1 K
inner dimensions: 40 cm x 34 cm x 40 cm (lxwxh)

Presi BRILLANT 200 – corundum wheel saw
ATM OPAL 410 – resin sample hot embedding
ATM SAPHIR 520 – polishing machine