MLZ is a cooperation between:

Technische Universität München> Technische Universität MünchenHelmholtz-Zentrum Hereon> Helmholtz-Zentrum Hereon
Forschungszentrum Jülich> Forschungszentrum Jülich

MLZ is a member of:

LENS> LENSERF-AISBL> ERF-AISBL

MLZ on social media:

Logo

MLZ (eng)

Lichtenbergstr.1
85748 Garching

SANS-1

Small angle neutron scattering instrument

This instrument is focussed on cold neutrons. Therefore, please carefully check the “Technical data WITHOUT cold source” section. Deviating parameters are in bold. The instrument team is happy to answer any further questions!

Insrumentscheme SANS-1 Insrumentscheme SANS-1

SANS-1 [1] is a standard pinhole instrument with a 23 m collimation distance and a 20 m sample detector distance.

The instrument is equipped with two interchangeable velocity selectors permitting 10 – 15 % or 5 – 10 % Δλ/λ and a 14-window double-disc chopper for TISANE. This combination allows versatile tuning of the flux, resolution, duty cycle, and frame overlap, including time-resolved measurements with repetition rates up to 10 kHz. A 150 kHz RF spin flipper and two V-cavity transmission polarisers provide polarised neutrons in SANSPOL and POLARIS set-ups in a broad wavelength band from 4.5 to 16 Å. A key feature is the large accessible dynamic Q-range facilitated by the sideways movement of the primary 1 m2 detector, particularly for single-shot measurements.

With its focus on materials science and magnetism, the flexibility of SANS-1 relies heavily on a spacious sample area. The new heavy-duty six-axes goniometer makes it possible to position almost any bulky and heavy sample environment up to 1000 kg weight, 125 × 250 cm2 in lateral and 300 cm in vertical size with a precision of 0.01 mm and 0.02°.

The sample area of SANS-1 is constructed out of non-magnetic materials wherever possible to allow for the use of the entire rage of superconducting magnets available at MLZ, also in combination with dilution inserts. The use of a non-shielded high field is possible. The sample goniometer also fulfils the rising demand for diffraction experiments at low scattering angles, e.g., for studies of superconducting vortex lattices and other large magnetically ordered systems.

[1] Mühlbauer, S. et al., NIM-A, 832, 297 (2016).

Typical applications

SANS-1 is dedicated to studying nanoscale length scales of 10 to 3000 Å, particularly adapted for the needs of materials research and magnetism. It allows hosting a wide range of different sample environments, including a bespoke dilatometer for in-situ rapid quenching/heating and stress analysis.

  • Precipitates and segregation in alloys
  • Rapid quenching/heating and deformation of alloys
  • Defects in materials, surfactants, colloids
  • Ferromagnetic correlations in magnetism
  • Anode materials and functionality of batteries
  • Magnetic domains & nanoparticles
  • Polymers, proteins, biological membranes, viruses, ribosomes and macromolecules
  • Superconducting vortex lattices
  • Large emergent magnetic structures such as helical magnets and skyrmion lattices

During thermal operation without the cold source, the focus will be on studies of shorter correlations up to 1000 Å in a mostly non-polarised set-up using shorter wavelengths and shorter collimation distances.

Sample environment
  • Standard sample changers with 22 positions, 11 positions for the magnet and 11 positions with thermostat (-10 – +200°C)
  • MLZ suite of high-temperature furnaces up to 1900°C
  • Deformation-rig with heating: 100 kN
  • Set of magnets (2.5 T and 5 T horizontal, 7.5 T vertical, 12 T vertical (TAS magnet))
  • MLZ suite of cryostats, including low-T inserts
  • Dilatometer DIL 805 A/D/T Quenching Dilatometer [2]
  • NB Nanoscale, D5 HF-Generator for magnetic hyperthermia [3]

[2] TA Instruments, DIL805A/D/T Quenching dilatometer
[3] NB Nanoscale, D5 HF-Generator for Magnetic Hyperthermia

Technical data WITHOUT cold source
Primary beam
  • Mechanical velocity selectors with variable speed
    • Δλ/λ = 10 – 20 % resolution
    • Δλ/λ = 6 – 16 % resolution
    • Wavelength range: 3.45 – 6 Å
Polarisation
  • Two V-shaped polarisers
Collimation system (source-to-sample distance)
  • 1 m, 2 m, 4 m, 8 m, 12 m, 16 m in steps via insertion of neutron guide sections
Sample size
  • 0 – 35 mm diameter
Q-range
  • 0.01 Å-1 < Q < 1 Å-1
Detectors
  • Primary detector: 1 m2 array of 128 3He position sensitive tubes with 8 mm resolution; SD 1 – 12 m; lateral detector movement up to 0.5 m, rate capability max. 2 MHz
Technical data WITH cold source
Primary beam
  • Mechanical velocity selectors with variable speed
    • Δλ/λ = 10 – 20 % resolution
    • Δλ/λ = 6 – 16 % resolution
    • Wavelength range: 3.45 – 20 Å
Polarisation
  • Two V-shaped polarisers
Collimation system (source-to-sample distance)
  • 1 m, 2 m, 4 m, 8 m, 12 m, 16 m, 20 m and 23 m in steps via insertion of neutron guide sections
Sample size
  • 0 – 35 mm diameter
Q-range
  • 0.002 Å-1 < Q < 1 Å-1
Detectors
  • Primary detector: 1 m2 array of 128 3He position sensitive tubes with 8 mm resolution; SD 1 – 20 m; lateral detector movement up to 0.5 m, rate capability max. 2 MHz

Instrument scientists

Dr. André Heinemann
Phone: +49 (0)89 289-14534
E-mail: andre.heinemann@hzg.de

Dr. Sebastian Mühlbauer
Phone: +49 (0)89 289-10784
E-mail: sebastian.muehlbauer@frm2.tum.de

SANS-1
Phone: +49 (0)89 289-12818

Operated by

TUM

GEMS

Funding

News

Tracing the hydrogen

Tracing the hydrogen

Read more
HYMN: A high-frequency setup on the road

HYMN: A high-frequency setup on the road

Read more
Let's quench!

Let's quench!

Read more

Publications

Find the latest publications regarding SANS-1 in our publication database iMPULSE:

impulse.mlz-garching.de

Citation of the instrument

Heinz Maier-Leibnitz Zentrum. (2015). SANS-1: Small angle neutron scattering. Journal of large-scale research facilities, 1, A10. http://dx.doi.org/10.17815/jlsrf-1-32

For citation please always include the DOI.

Instrument control

Gallery

SANS-1
SANS-1
© W. Schürmann, TUM
SANS-1
SANS-1

View into the collimation chamber of the SANS-1

© MLZ

MLZ is a cooperation between:

Technische Universität München> Technische Universität MünchenHelmholtz-Zentrum Hereon> Helmholtz-Zentrum Hereon
Forschungszentrum Jülich> Forschungszentrum Jülich

MLZ is a member of:

LENS> LENSERF-AISBL> ERF-AISBL

MLZ on social media: